HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 613483Generated: October 29, 2026
Dimethylformamide → HCID 19592550, compound
https://huagongshe.com/reaction/613483
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | 2-Methoxyethylamine | HCID 8018 | — |
| Reactant | 4-Chloro-8-(2,6-dichlorobenzoylamino)quinoline | HCID 19592564 | — |
| Product | HCID 19592550 | HCID 19592550 | — |
Reaction Steps
A mixture of 4-chloro-8-(2,6-dichlorobenzoylamino)quinoline (130 mg) and 2-methoxyethylamine (210 mg) in dimethylformamide (1.5 ml) was heated for 5 hours at 100° C. The mixture was concentrated in vacuo, and the residue was purified by preparative thin layer chromatography to give 8-(2,6-dichlorobenzoylamino)-4-dimethylaminoquinoline (94 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06008230 |
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| Source dataset | uspto-grants-1999_12 |
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| ORD ID | ord-4e823b747644468ca8b9f7f3f81edbd3 |
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| Source note | uspto-grants-1999_12 |
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