HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 613546Generated: October 31, 2026
Hydrazine hydrate (1:1) → HCID 19592850, compound
https://huagongshe.com/reaction/613546
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | 4-Chloro-8-(2,6-dichlorobenzoylamino)quinoline | HCID 19592564 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | HCID 19592850 | HCID 19592850 | 87.6% |
Reaction Steps
A mixture of 4-chloro-8-(2,6-dichlorobenzoylamino)quinoline (200 mg) and hydrazine monohydrate (285 mg) in ethanol (4 ml) and N-methylpyrrolidone (1 ml) was heated at 100° C. overnight. After cooling, the resulting precipitates were collected by filtration, and the residue was recrystallized from ethanol to give 8-(2,6-dichlorobenzoylamino)-4-hydrazinoquinoline (173 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06008230 |
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| Source dataset | uspto-grants-1999_12 |
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| ORD ID | ord-83ac8aead5504492aafd71d3ce9ff309 |
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| Source note | uspto-grants-1999_12 |
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