Chlorotrifluoroethylene → HCID 23237106, compound

HRID 613801Notes

Reaction equation

HRID 613801 reaction equation
[Cl:1][C:2]([F:6])=[C:3]([F:5])[F:4].[CH2:7]=[CH:8][CH:9]=[CH2:10]>>[Cl:1][C:2]1([F:6])[C:3]([F:5])([F:4])[CH2:10][CH:9]=[CH:8][CH2:7]1

Participants

3

Reactant 2

HCID 6594ChlorotrifluoroethyleneHCID 78451,3-Butadiene

Product 1

HCID 23237106HCID 23237106, compound

Procedure

4-chloro-4,5,5-trifluorocyclohexene was prepared in the same manner as in Example 12 except that chlorotrifluoroethylene (CTFE) and 1,3-butadiene were continuously injected into the flow reactor at the rates of 65.2 g/hr and 30.3 g/hr, respectively. Then, 8.6 g of unreacted chlorotrifluoroethylene (CTFE) was recovered. The resultant was purified by steam distillation, and then the water layer was removed to give 64.9 g of the mixture (GC%=61%).

Workup

  1. customThen, 8.6 g of unreacted chlorotrifluoroethylene (CTFE) was recovered
  2. distillationThe resultant was purified by steam distillation
  3. customthe water layer was removed

Sources & evidence

ORD record
ord-159a7e97243245ef94e4260a64b45480
Source dataset
uspto-grants-1999_12
Patent number
US06008407

Reaction notes

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