Chlorotrifluoroethylene → HCID 23237106, compound

Participants

Reaction Steps

4-chloro-4,5,5-trifluorocyclohexene was prepared in the same manner as in Example 12 except that chlorotrifluoroethylene (CTFE) and 1,3-butadiene were continuously injected into the flow reactor at the rates of 65.2 g/hr and 30.3 g/hr, respectively. Then, 8.6 g of unreacted chlorotrifluoroethylene (CTFE) was recovered. The resultant was purified by steam distillation, and then the water layer was removed to give 64.9 g of the mixture (GC%=61%).

Provenance & Evidence