Chlorotrifluoroethylene → HCID 23237106, compound

HRID 613802Notes

Reaction equation

HRID 613802 reaction equation
[Cl:1][C:2]([F:6])=[C:3]([F:5])[F:4].[CH2:7]=[CH:8][CH:9]=[CH2:10]>>[Cl:1][C:2]1([F:6])[C:3]([F:5])([F:4])[CH2:10][CH:9]=[CH:8][CH2:7]1

Participants

3

Reactant 2

HCID 6594ChlorotrifluoroethyleneHCID 78451,3-Butadiene

Product 1

HCID 23237106HCID 23237106, compound

Procedure

4-chloro-4,5,5-trifluorocyclohexene was prepared in the same manner as in Comparative Example 4 except that chlorotrifluoroethylene (CTFE), 1,3-butadiene and nitrogen gas were continuously injected into the flow reactor in the rates of 33.8 g/hr, 15.7 g/hr, and 0.4 mol/hr, respectively. Then, 4.7 g of unreacted chlorotrifluoroethylene (CTFE) was recovered. The resultant was purified by steam distillation, and then the water layer was removed to give 29.4 g of the mixture (GC%=53%).

Workup

  1. customThen, 4.7 g of unreacted chlorotrifluoroethylene (CTFE) was recovered
  2. distillationThe resultant was purified by steam distillation
  3. customthe water layer was removed

Sources & evidence

ORD record
ord-50004c15bab64ef39c52a5a73932a240
Source dataset
uspto-grants-1999_12
Patent number
US06008407

Reaction notes

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