Chlorotrifluoroethylene → HCID 23237106, compound

Participants

Reaction Steps

4-chloro-4,5,5-trifluorocyclohexene was prepared in the same manner as in Comparative Example 4 except that chlorotrifluoroethylene (CTFE), 1,3-butadiene and nitrogen gas were continuously injected into the flow reactor in the rates of 33.8 g/hr, 15.7 g/hr, and 0.4 mol/hr, respectively. Then, 4.7 g of unreacted chlorotrifluoroethylene (CTFE) was recovered. The resultant was purified by steam distillation, and then the water layer was removed to give 29.4 g of the mixture (GC%=53%).

Provenance & Evidence