HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyanide → HCID 21329842, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyanide | HCID 5975 | — |
| Reactant | N-Ethyl cyclohexylamine | HCID 21609 | — |
| Reactant | 1,2-Dichloro-4-(2-isocyanatopropan-2-yl)benzene | HCID 21329862 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 21329842 | HCID 21329842 | 72.8% |
Reaction Steps
A solution of 2.3 g of 3,4-dichloro-α,α-dimethylbenzyl isocyanate, prepared from the corresponding cyanide in the same way as in Synthesis Example 1, in 10 ml of chloroform was added to 1.5 g of N-ethylcyclohexylamine. The solvent was then removed by distillation and the resulting white crystals were recrystallized from a mixture of benzene-n-hexane to obtain 2.6 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04143061 |
| Source dataset | uspto-grants-1979_03 |
| ORD ID | ord-2f7022194ad341769555256ad35a1077 |
| Source note | uspto-grants-1979_03 |