HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Ethyl cyclohexylamine → HCID 21329852, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Ethyl cyclohexylamine | HCID 21609 | — |
| Reactant | HCID 21329848 | HCID 21329848 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 21329852 | HCID 21329852 | 87.7% |
Reaction Steps
A solution of 1.8 g of p-fluoro-α,α-dimethylbenzyl isocyanate in 20 ml of n-hexane was added to 1.4 g of N-ethylcyclohexylamine, and the mixture was allowed to stand overnight. The solvent was then removed by distillation and the resulting crystals were washed with cold n-pentane to obtain 2.7 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04143061 |
| Source dataset | uspto-grants-1979_03 |
| ORD ID | ord-ec1af4fb194243a49ed15e7dd2ee8549 |
| Source note | uspto-grants-1979_03 |