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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 614028Generated: October 30, 2026

Cyanide → HCID 21329855, compound

https://huagongshe.com/reaction/614028

Reaction equation

Participants

RoleNameHCIDCharge
ReactantCyanideHCID 5975—
ReactantN-MethylanilineHCID 7515—
ReactantHCID 21329846HCID 21329846—
ProductHCID 21329855HCID 2132985586.4%

Reaction Conditions

Temperature60 °C

Reaction Steps

2.4 g of m-bromo-α,α-dimethylbenzyl isocyanate, prepared from the corresponding cyanide in the same way as in Synthesis Example 1, was added to 1.1 g of N-methylaniline and the mixture was heated at 60° C. for 2 hours. After allowing the reaction mixture to cool, the precipitated white crystals were separated by filtration and washed with n-hexane to obtain 3.0 g of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04143061
Source datasetuspto-grants-1979_03
ORD IDord-487f2e0f60a54abebef403c4ac9e1ed0
Source noteuspto-grants-1979_03