Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Cyanide | HCID 5975 | — |
| Reactant | N-Methylaniline | HCID 7515 | — |
| Reactant | HCID 21329846 | HCID 21329846 | — |
| Product | HCID 21329855 | HCID 21329855 | 86.4% |
Reaction Steps
2.4 g of m-bromo-α,α-dimethylbenzyl isocyanate, prepared from the corresponding cyanide in the same way as in Synthesis Example 1, was added to 1.1 g of N-methylaniline and the mixture was heated at 60° C. for 2 hours. After allowing the reaction mixture to cool, the precipitated white crystals were separated by filtration and washed with n-hexane to obtain 3.0 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04143061 |
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| Source dataset | uspto-grants-1979_03 |
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| ORD ID | ord-487f2e0f60a54abebef403c4ac9e1ed0 |
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| Source note | uspto-grants-1979_03 |
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