HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Cyanide → 4-Ethoxybenzene-1-carbonyl cyanide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Cyanide | HCID 9032 | — |
| Reactant | 4-Ethoxybenzoyl Chloride | HCID 140059 | — |
| Catalyst | HCID 178418546 | HCID 178418546 | — |
| Product | 4-Ethoxybenzene-1-carbonyl cyanide | HCID 23336274 | 94.5% |
Reaction Steps
In the manner described above, 184 g (1 mol) of p-ethoxybenzoyl chloride, 62.5 g (0.96 mol) of potassium cyanide and 3.6 g (0.04 mol) of copper(I) cyanide were reacted with one another at 215° C. After working up, 159 g (91% of theory) of p-ethoxybenzoyl cyanide were obtained; melting point 43° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04143068 |
| Source dataset | uspto-grants-1979_03 |
| ORD ID | ord-7a7d4285c3a8478c8cabc3b9d3f37da6 |
| Source note | uspto-grants-1979_03 |