HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21330005, compound → HCID 21330002, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21330005 | HCID 21330005 | — |
| Reactant | Acetic Acid Mixture with Hydrobromic Acid | HCID 21893785 | — |
| Product | HCID 21330002 | HCID 21330002 | — |
Reaction Steps
40 g 1-(1-carbobenzoxyaminoethyl)-3,4-dihydro-6,7-dimethoxyisoquinoline are dissolved in 450 ml 40% HBr/acetic acid. The mixture is maintained at room temperature for 1 hour and then concentrated in a vacuum to give a crystalline residue of 1-(1-aminoethyl)-3,4-dihydro-6,7-dimethoxyisoquinoline dihydrobromide which is washed with ether before further use (M.Pt. 234°-235°).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04143143 |
| Source dataset | uspto-grants-1979_03 |
| ORD ID | ord-ab217360f72044cd84b88f326ff6e7ac |
| Source note | uspto-grants-1979_03 |