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HRID614152

反应详情

EQUATION

反应方程式

HRID 614152 的结构方程式

REACTANTS

反应物

3
结构：[Br-].[K+]
HCID253877

Potassium bromide

BrK

结构：CCOC(=O)C=C(C)NCC(=O)[O-].[Na+]
HCID86736030

未命名化合物

结构：CC1(C)S[C@@H]2C(NC(=O)C(N)c3ccc(O)cc3)C(=O)N2C1c1nnn[nH]1
HCID178431937

未命名化合物

PRODUCTS

生成物

1
结构：CC1(C)S[C@@H]2C(NC(=O)C(NC(=O)CN)c3ccc(O)cc3)C(=O)N2C1c1nnn[nH]1
HCID178431940

未命名化合物

收率 45%

PROCEDURE

实验过程

The title compound is prepared in 45% yield from 6-(2-amino-2-[p-hydroxyphenyl]acetamido)-2,2-dimethyl-3-(5-tetrazolyl)penam and sodium N-(2-ethoxycarbonyl-1-methylvinyl)-2-aminoacetate, using the procedure of Example XC. The product has m.p. 173°-188° C. (dec.) IR (KBr disc): 1785 cm-1 (β-lactam). NMR (DMSO-d6): 7.55-7.10 ppm (m, 2H), 7.00-6.00 ppm (m, 2H), 5.75-5.40 ppm (m, 3H), 5.10 ppm (s, 1H), 3.65 ppm (m, 2H), 1.55 ppm (s, 3H), 0.95 ppm (s, 3H).