HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → glycyl-L-phenylalanine benzyl ester hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 7408191 | HCID 7408191 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | glycyl-L-phenylalanine benzyl ester hydrochloride | HCID 70603822 | — |
Reaction Steps
13.4 Parts N-t-butoxycarbonylglycyl-L-phenylalanine benzyl ester is dissolved in 200 parts dioxane and treated with a 10 fold excess of 2 N hydrochloric acid in dioxane for 10 minutes. Removal of the solvent under reduced pressure affords pure glycyl-L-phenylalanine benzyl ester hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04144228 |
| Source dataset | uspto-grants-1979_03 |
| ORD ID | ord-a147c1413df543ebb37d2a026621977a |
| Source note | uspto-grants-1979_03 |