huagongshe.com
HRID614202

反应详情

EQUATION

反应方程式

HRID 614202 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CC(C)(C)OC(=O)NCC(=O)N[C@@H](Cc1ccccc1)C(=O)OCc1ccccc1
HCID7408191

未命名化合物

PRODUCTS

生成物

1
结构：Cl.NCC(=O)N[C@@H](Cc1ccccc1)C(=O)OCc1ccccc1
HCID70603822

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1COCCO1
溶剂HCID31275

1,4-Dioxane

C4H8O2

2 次

PROCEDURE

实验过程

13.4 Parts N-t-butoxycarbonylglycyl-L-phenylalanine benzyl ester is dissolved in 200 parts dioxane and treated with a 10 fold excess of 2 N hydrochloric acid in dioxane for 10 minutes. Removal of the solvent under reduced pressure affords pure glycyl-L-phenylalanine benzyl ester hydrochloride.

WORKUP

后处理

  1. customRemoval of the solvent under reduced pressure