4-Chlororesorcinol → HCID 131711456, compound

HRID 614298Notes

Reaction equation

[Cl:1][C:2]1[CH:8]=[CH:7][C:5]([OH:6])=[CH:4][C:3]=1[OH:9].[OH-].[Na+].[CH2:12]1[O:15][CH:13]1[CH3:14]>>[Cl:1][C:2]1[CH:8]=[CH:7][C:5]([OH:6])=[CH:4][C:3]=1[OH:9].[CH2:12]1[O:15][CH:13]1[CH3:14]

Participants

Reactant 3

HCID 17314-Chlororesorcinol

HCID 6378Propylene Oxide

HCID 14798Sodium Hydroxide

Product 1

HCID 131711456HCID 131711456, compound

Procedure

One hundred and nineteen (119) parts of 4-chlororesorcine and 1.0 part of sodium hydroxide were reacted with 581 parts of propylene oxide at not higher than 5 kg/cm2, at 140°-170° C. for 40 minutes to obtain a 4-chlororesorcine-propylene oxide adduct (the average amount added, n=8) which was a light-yellow viscous liquid.

Sources & evidence

ORD record: ord-9653be678fa94e13ac6204645ff8f4c0
Source dataset: uspto-grants-1979_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04144283

Reaction notes

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