HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Dimethylethylenediamine → HCID 23349902, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Dimethylethylenediamine | HCID 66053 | — |
| Reactant | 4-methoxypyrimidine | HCID 303830 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 23349902 | HCID 23349902 | — |
Reaction Steps
A solution of 4-methoxypyrimidine (12.9 g., 0.117 mole) and unsym-dimethylethylene diamine (20.7 g., 0.23 mole) in 40 ml of xylene is heated under reflux for 64 hours. The reaction is concentrated and the oil is distilled at 15 mm of Hg. 4-(2-Dimethylaminoethylamino)pyrimidine, boiling at 164°-169° C., is collected.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04144338 |
| Source dataset | uspto-grants-1979_03 |
| ORD ID | ord-1bb734a4478a4fed8bce03b403cd9c07 |
| Source note | uspto-grants-1979_03 |