HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 86736397, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 21329357 | HCID 21329357 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 86736397 | HCID 86736397 | — |
Reaction Steps
A mixture of nicotinoyl hydrazine-N-oxide (25.3 g; 0.166 m), acetic acid (85 ml) and acetic anhydride (16.9 g; 0.166 m) was heated at reflux. After one hour, the reaction mixture was cooled and poured into diethylether to yield 32 g of N-acetylnicotinoylhydrazine N-oxide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04144343 |
| Source dataset | uspto-grants-1979_03 |
| ORD ID | ord-b49e261eb629456ca553c5d651bbd905 |
| Source note | uspto-grants-1979_03 |