HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Hydroxide → HCID 12445400, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | N-(2-Fluorophenyl)-3,5-dinitropyridin-2-amine | HCID 12445387 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12445400 | HCID 12445400 | — |
Reaction Steps
A mixture of the product from Step A (1.0 g.) 15 ml. of ethanol and 5 ml. of concentrated ammonium hydroxide was warmed to 70° C. and hydrogen sulfide was bubbled in for 20 minutes. After cooling, the precipitate was collected and recrystallized from ethanol to give 2-(2-fluoroanilino)-3-amino-5-nitropyridine, m.p. 171°-172° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04144341 |
| Source dataset | uspto-grants-1979_03 |
| ORD ID | ord-f45c0cf662834a72af9a2dcbdb8caf92 |
| Source note | uspto-grants-1979_03 |