HRID614344

反应详情

EQUATION

反应方程式

HRID 614344 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of 431 mg. of 1,3-dihydro-3-(3,4-methylenedioxyphenyl)-1-phenacylimidazo[4,5-b]pyridin-2-one in 30 ml. of methanol was hydrogenated over 25 mg. of platinum oxide. The catalyst was removed by filtration and the filtrate was evaporated to dryness to give a glass which could not be crystallized.

WORKUP

后处理

  1. additionA mixture of 431 mg
  2. customThe catalyst was removed by filtration
  3. customthe filtrate was evaporated to dryness
  4. customto give a glass which could not
  5. custombe crystallized