HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 21329390, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 3-Chloro-N,N-dimethyl-1-propanamine | HCID 66960 | — |
| Reactant | HCID 21329388 | HCID 21329388 | — |
| Product | HCID 21329390 | HCID 21329390 | — |
Reaction Steps
A mixture of 21.7g (0.1 mole) of 1,2,4,5,6,7-hexahydrothiocino-[5,4-b]indole, 4.29g (0.102 mole) of 57% dispersion sodium hydride and 12.16g (0.1 mole) of 3-dimethylaminopropyl chloride is treated according to the procedure in Example 6. Recrystallization from pentane affords 20.5g (68%) of an analytical sample, m.p. 70°-71° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04144349 |
| Source dataset | uspto-grants-1979_03 |
| ORD ID | ord-45fceb81f5e947c9ad2e78754690b9db |
| Source note | uspto-grants-1979_03 |