HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 21329394, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 3-Chloro-N,N-dimethyl-1-propanamine | HCID 66960 | — |
| Reactant | HCID 21329392 | HCID 21329392 | — |
| Product | HCID 21329394 | HCID 21329394 | — |
Reaction Steps
A mixture of 9.0g (0.0276 mole) of 1,2,4,5,6,7-hexahydro-10-bromothiocino[5,4-b]indole 3,3-dioxide, 1.3g (0.03 mole) of 57% dispersion sodium hydride and 3.36g (0.0276 mole) of 3-dimethylaminopropyl chloride is treated according to the procedure in Example 6. After recrystallization from ethyl acetate, there is obtained 6.0g (52%) of an analytical sample, m.p. 135°-137° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04144349 |
| Source dataset | uspto-grants-1979_03 |
| ORD ID | ord-1f71092fa046494eb0b1d072c7c68f9e |
| Source note | uspto-grants-1979_03 |