HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70572688, compound → HCID 21315520, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70572688 | HCID 70572688 | — |
| Reactant | HCID 86736414 | HCID 86736414 | — |
| Reactant | 1H-Dibenz[2,3:6,7]oxepino[4,5-c]pyrrole, 5-chloro-2,3,3a,12b-tetrahydro-2-methyl-, (3aR,12bS)-rel-, (2Z)-2-butenedioate (1:1) | HCID 86736415 | — |
| Reactant | HCID 86736416 | HCID 86736416 | — |
| Reactant | HCID 86736418 | HCID 86736418 | — |
| Product | HCID 21315520 | HCID 21315520 | — |
Reaction Steps
cis-2-methyl-2,3,3a,12b-tetrahydro-1H-dibenz[2,3;6,7] oxepino[4,5-c]pyrrole maleate, m.p. 143-144° C.; cis-2,5-dimethyl-2,3,3a,12b-tetrahydro-1H-dibenz[ 2,3;6,7]oxepino[4,5-c]pyrrole, m.p. 99-101° C.; cis-2-methyl-5-chloro-2,3,3a,12b-tetrahydro-1H-dibenz[ 2,3;6,7]oxepino[4,5-c]pyrrole maleate, m.p. 116-169° C.; cis-2-methyl-1,2,3,4,4a,13b-hexahydro-dibenz[2,3;6,7] oxepino[4,5-c]pyridine maleate, m.p. 174-1750° C.; cis-2-methyl-2,3,4,4a,9,13b-hexahydro-1H-dibenzo[1,2;5,6] cyclohepta[3,4-c]pyridine maleate, m.p. 207-209° C. and the corresponding trans isomer (maleate salt), m.p. 175-176° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04145434 |
| Source dataset | uspto-grants-1979_03 |
| ORD ID | ord-ac7e75df02ff4a7bbf4464610f11502d |
| Source note | uspto-grants-1979_03 |