HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Hydroxide → 1-Methyl-3-nitro-1H-pyrazole-4-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | 1-Methyl-3-nitro-1H-pyrazole-4-carbonyl chloride | HCID 23329508 | — |
| Product | 1-Methyl-3-nitro-1H-pyrazole-4-carboxamide | HCID 21161920 | — |
Reaction Steps
Seven gm. of 1-methyl-3-nitro-4-pyrazolecarbonyl chloride was added in portions to 50 ml. of concentrated NH4OH. The mixture was heated at reflux for 15 to 20 minutes, evaporated to dryness, and cooled. The resultant crystallized product was identified as 1-methyl-3-nitro-4-pyrazolecarboxamide, m.p. 190°-192° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04145554 |
| Source dataset | uspto-grants-1979_03 |
| ORD ID | ord-6b471832dc034e19acc5665c334a8142 |
| Source note | uspto-grants-1979_03 |