HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 21327245, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Isoamyl Nitrite | HCID 8053 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | HCID 21327278 | HCID 21327278 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 21327245 | HCID 21327245 | — |
Reaction Steps
This is obtained by nitrosation and subsequent ring closure by treating 2-(2-acetoxyethyl)-3-acetamidophenyl benzyl ether with isoamyl nitrite, sodium acetate and acetic anhydride in toluene at 80° C. It is obtained in the form of colorless crystals; m.p. 99°-100° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04146630 |
| Source dataset | uspto-grants-1979_03 |
| ORD ID | ord-ca3f49e8eeb740218775e6f47c2e4b55 |
| Source note | uspto-grants-1979_03 |