Hydrochloric Acid → HCID 70506019, compound

HRID 615047Notes

Reaction equation

HRID 615047 reaction equation
[CH2:1]([NH:17][C:18]1[CH:26]=[CH:25][C:21]([C:22]([OH:24])=[O:23])=[CH:20][CH:19]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16].[ClH:27]>C(Cl)Cl>[ClH:27].[CH2:1]([NH:17][C:18]1[CH:19]=[CH:20][C:21]([C:22]([OH:24])=[O:23])=[CH:25][CH:26]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 472634-(Hexadecylamino)benzoic acid

Product 1

HCID 70506019HCID 70506019, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

A solution of 2.00 g of 4-(n-hexadecylamino)benzoic acid in 80 ml of methylene chloride is stirred at 35° C. and treated with anhydrous hydrogen chloride. The resulting mixture is chilled and filtered to yield 4-(n-hexadecylamino)benzoic acid hydrochloride as a white solid.

Workup

  1. temperatureThe resulting mixture is chilled
  2. filtrationfiltered

Sources & evidence

ORD record
ord-d120f3a58b264a52873f72b99fb08d8d
Source dataset
uspto-grants-1979_03
Patent number
US04146546

Reaction notes

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