Diethylamine → HCID 13090789, compound

HRID 615070Notes

Reaction equation

HRID 615070 reaction equation
[Cl:1][C:2]1[CH:3]=[N:4][C:5]2[C:10]([CH:11]=1)=[CH:9][CH:8]=[C:7]([Cl:12])[C:6]=2[CH2:13]Cl.[CH2:15]([NH:17][CH2:18][CH3:19])[CH3:16]>O>[Cl:1][C:2]1[CH:3]=[N:4][C:5]2[C:10]([CH:11]=1)=[CH:9][CH:8]=[C:7]([Cl:12])[C:6]=2[CH2:13][N:17]([CH2:18][CH3:19])[CH2:15][CH3:16]

Participants

4

Reactant 2

HCID 8021DiethylamineHCID 13090784HCID 13090784, compound

Product 1

HCID 13090789HCID 13090789, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

24.6 parts of 3,7-dichloro-8-chloromethylquinoline and 30 parts of diethylamine were stirred at 55° C. for 6 hours. Water was added and the solid was filtered off with suction and dried. 25 parts of 3,7-dichloro-8-diethylaminomethylquinoline of melting point 54° C. were obtained. The yield corresponds to 89% of theory.

Workup

  1. filtrationthe solid was filtered off with suction
  2. customdried

Sources & evidence

ORD record
ord-10d20af6330a49038d3c50d2204a5937
Source dataset
uspto-grants-1985_02
Patent number
US04497651

Reaction notes

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