Acetone → HCID 13454040, compound

HRID 615082Notes

Reaction equation

HRID 615082 reaction equation
[NH2:1][C:2]1[NH:3][C:4]2[CH:10]=[CH:9][CH:8]=[CH:7][C:5]=2[N:6]=1.[CH:11]([N:14]=[C:15]=[O:16])([CH3:13])[CH3:12].[CH3:17][C:18]([CH3:20])=O>>[CH3:12][C:11]1([CH3:13])[N:14]([CH:18]([CH3:20])[CH3:17])[C:15](=[O:16])[N:6]2[C:2]([N:3]([C:15]([NH:14][CH:11]([CH3:13])[CH3:12])=[O:16])[C:4]3[CH:10]=[CH:9][CH:8]=[CH:7][C:5]=32)=[N:1]1

Participants

4

Reactant 3

HCID 180AcetoneHCID 136242-AminobenzimidazoleHCID 61277Isopropyl isocyanate

Product 1

HCID 13454040HCID 13454040, compound

Procedure

The title compound was prepared from 2-aminobenzimidazole, acetone and isopropyl isocyanate employing the method of the first paragraph of Example 1. The product was purified by column chromatography on silica, eluting with chloroform to give a white solid, mp 80°-89° C. The confirmatory elemental analysis is shown in Table III.

Workup

  1. customThe product was purified by column chromatography on silica
  2. washeluting with chloroform
  3. customto give a white solid, mp 80°-89° C

Sources & evidence

ORD record
ord-cac77732e26e4144a29bf3c16817678b
Source dataset
uspto-grants-1985_02
Patent number
US04497650

Reaction notes

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