Hydrochloric Acid → HCID 70479626, compound

HRID 615193Notes

Reaction equation

HRID 615193 reaction equation
[ClH:1].[CH:2]1([NH:8][C@@H:9]2[CH2:26][C@@:24]3([CH3:25])[C@@H:20]([CH2:21][CH2:22][C@@H:23]3[C:27]([O:29][CH3:30])=[O:28])[C@H:19]3[C@H:10]2[C@:11]2([CH3:33])[C@@H:16]([CH2:17][CH2:18]3)[CH2:15][C@H:14]([OH:31])[C@@H:13]([OH:32])[CH2:12]2)[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1>O>[ClH:1].[CH:2]1([NH:8][C@@H:9]2[CH2:26][C@@:24]3([CH3:25])[C@@H:20]([CH2:21][CH2:22][C@@H:23]3[C:27]([O:29][CH3:30])=[O:28])[C@H:19]3[C@H:10]2[C@:11]2([CH3:33])[C@@H:16]([CH2:17][CH2:18]3)[CH2:15][C@H:14]([OH:31])[C@@H:13]([OH:32])[CH2:12]2)[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7]1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 70479340HCID 70479340, compound

Product 1

HCID 70479626HCID 70479626, compoundYield 2%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

A solution (11.4 ml; 0.0979M) of HCl in water was added to the product of Example 3 (500 mg) and the mixture stirred until a clear solution was obtained. The solution was made up to 25 g with water to give a 2% solution with pH 2.7.

Workup

  1. customwas obtained

Sources & evidence

ORD record
ord-0c0abd852fd24d27a456ba5e3b1f8763
Source dataset
uspto-grants-1985_02
Patent number
US04497805

Reaction notes

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