HRID615263

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID70370

2,6-Di-tert-butyl-4-mercaptophenol

C14H22OS

$结构：COC(=O)/C=C\C(=O)OC$

HCID5271565

Dimethyl maleate

C6H8O4

PRODUCTS

生成物

结构：COC(=O)CC(Sc1cc(C(C)(C)C)c(O)c(C(C)(C)C)c1)C(=O)OC

HCID20255224

未命名化合物

收率 80%

AUXILIARIES

试剂、催化剂与溶剂

催化剂HCID8471

Triethylamine

C6H15N

PROCEDURE

实验过程

The procedure of Example 1 is repeated using 23.84 grams of 2,6-di-tert-butyl-4-mercaptophenol, 14.41 grams of dimethyl maleate, and 0.5 grams of triethylamine. The product is recrystallized from heptane to give 30.44 grams (80% yield) of white solid, m.p. 94°-96° C.

WORKUP

后处理

customThe product is recrystallized from heptane