HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → 1,3,5-Triazino(1,2-a)benzimidazol-4(1H)-one, 2,3-dihydro-2,2-dimethyl-3-propyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 13454039 | HCID 13454039 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 1,3,5-Triazino(1,2-a)benzimidazol-4(1H)-one, 2,3-dihydro-2,2-dimethyl-3-propyl- | HCID 159104 | — |
Reaction Steps
The title compound was prepared by hydrolysis of the precursor compound of Example 3 in the presence of 10% aqueous sodium hydroxide and THF employing the method of paragraph 2, Example 1. The product was crystallized from acetone to give colorless prisms, mp 170° C. (dec). The confirmatory elemental analysis is shown in Table III.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04498920 |
| Source dataset | uspto-grants-1985_02 |
| ORD ID | ord-b86ccace22aa47c595405d470099ef1c |
| Source note | uspto-grants-1985_02 |