HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-6-methoxybenzothiazole → HCID 70487283, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-6-methoxybenzothiazole | HCID 15630 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Reactant | Iodomethyl pivalate | HCID 104401 | — |
| Product | HCID 70487283 | HCID 70487283 | — |
Reaction Steps
A solution of 2-amino-6-methoxy benzothiazole (8.5 g) and iodomethyl pivalate (11.5 g) in dry dioxan (120 ml) was stored at room temperature for 7 days. The resulting solid was collected and dried to give the sub-title product (14 g), mp 191°-3° as a hemi-solvate with dioxan (n.m.r.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04499269 |
| Source dataset | uspto-grants-1985_02 |
| ORD ID | ord-5616e278f0c847bea8590786c702472c |
| Source note | uspto-grants-1985_02 |