Acetyl chloride → HCID 20256343, compound

HRID 615640Notes

Reaction equation

HRID 615640 reaction equation
[CH3:1][N:2]([CH3:22])[CH2:3][CH2:4][NH:5][C:6](=[O:21])[N:7]([CH:18]([CH3:20])[CH3:19])[CH2:8][CH2:9][O:10][C:11]1[CH:16]=[CH:15][C:14]([NH2:17])=[CH:13][CH:12]=1.CC(N([CH2:30][CH2:31][O:32]C1C=CC(N)=CC=1)C(N)=O)C.C(Cl)(=O)C>C(N(CC)CC)C>[CH3:22][N:2]([CH3:1])[CH2:3][CH2:4][NH:5][C:6](=[O:21])[N:7]([CH:18]([CH3:19])[CH3:20])[CH2:8][CH2:9][O:10][C:11]1[CH:12]=[CH:13][C:14]([NH:17][C:31](=[O:32])[CH3:30])=[CH:15][CH:16]=1

Participants

5

Reactant 3

HCID 6367Acetyl chlorideHCID 20256268HCID 20256268, compoundHCID 86739924HCID 86739924, compound

Product 1

HCID 20256343HCID 20256343, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

The title compound is prepared by reacting the compound of Example 64: N'-[2-dimethylamino)ethyl]-N-(1-methylethyl)-N-[2-(4-aminophenoxy)ethyl]urea with acetyl chloride in triethylamine.

Sources & evidence

ORD record
ord-00956f9cfb7a4a399c7dc0ded82f85b0
Source dataset
uspto-grants-1985_02
Patent number
US04500529

Reaction notes

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