Benzoyl chloride → HCID 20256307, compound

HRID 615641Notes

Reaction equation

HRID 615641 reaction equation
[CH3:1][N:2]([CH3:22])[CH2:3][CH2:4][NH:5][C:6](=[O:21])[N:7]([CH:18]([CH3:20])[CH3:19])[CH2:8][CH2:9][O:10][C:11]1[CH:16]=[CH:15][C:14]([NH2:17])=[CH:13][CH:12]=1.[C:23](Cl)(=[O:30])[C:24]1[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1>C(N(CC)CC)C>[C:23]([NH:17][C:14]1[CH:13]=[CH:12][C:11]([O:10][CH2:9][CH2:8][N:7]([CH:18]([CH3:19])[CH3:20])[C:6]([NH:5][CH2:4][CH2:3][N:2]([CH3:1])[CH3:22])=[O:21])=[CH:16][CH:15]=1)(=[O:30])[C:24]1[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1

Participants

4

Reactant 2

HCID 7412Benzoyl chlorideHCID 20256268HCID 20256268, compound2×

Product 1

HCID 20256307HCID 20256307, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

The title compound is prepared by reacting the compound of Example 64: N'-[2-(dimethylamino)ethyl]-N-(1-methylethyl)-N-[2-(4-aminophenoxy)ethyl]urea with benzoyl chloride in triethylamine.

Sources & evidence

ORD record
ord-e71dacd5da0d4b48ba7a7169470a52ad
Source dataset
uspto-grants-1985_02
Patent number
US04500529

Reaction notes

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