HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 23318282, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | N-[5-tert-Butyl-4-(hexadecyloxy)-2-hydroxyphenyl]acetamide | HCID 20257269 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23318282 | HCID 23318282 | — |
Reaction Steps
A mixture of 23.0 g of 2-acetylamino-4-tert-butyl-5-hexadecyloxyphenol, 120 ml of ethanol and 96 ml of 35% hydrochloric acid was refluxed with stirring for 5 hours. The reaction solution was cooled to precipitate crystals. The crystals were collected by filtration. 23.2 g of 2-amino-4-tert-butyl-5-hexadecyloxyphenol hydrochloride was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04500626 |
| Source dataset | uspto-grants-1985_02 |
| ORD ID | ord-514f93dd219045f089d63056bf10c5d0 |
| Source note | uspto-grants-1985_02 |