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HRID615656

反应详情

EQUATION

反应方程式

HRID 615656 的结构方程式

REACTANTS

反应物

2
反应SMILES：Cl
HCID313

Hydrochloric Acid

ClH

反应SMILES：CCCCCCCCCCCCCCCCOc1cc(O)c(NC(C)=O)cc1C(C)(C)C
HCID20257269

N-[5-tert-Butyl-4-(hexadecyloxy)-2-hydroxyphenyl]acetamide

C28H49NO3

PRODUCTS

产物

1
反应SMILES：CCCCCCCCCCCCCCCCOc1cc(O)c(N)cc1C(C)(C)C.Cl
HCID23318282

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
反应SMILES：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

A mixture of 23.0 g of 2-acetylamino-4-tert-butyl-5-hexadecyloxyphenol, 120 ml of ethanol and 96 ml of 35% hydrochloric acid was refluxed with stirring for 5 hours. The reaction solution was cooled to precipitate crystals. The crystals were collected by filtration. 23.2 g of 2-amino-4-tert-butyl-5-hexadecyloxyphenol hydrochloride was obtained.

WORKUP

后处理

  1. temperaturewas refluxed
  2. temperatureThe reaction solution was cooled
  3. customto precipitate crystals
  4. filtrationThe crystals were collected by filtration