Carbon Dioxide → HCID 11499277, compound

HRID 615671Notes

Reaction equation

HRID 615671 reaction equation
[C:1](=[O:3])=[O:2].[NH:4]([CH2:8][CH2:9][OH:10])[CH2:5][CH2:6][OH:7].O>>[C:1](=[O:7])([OH:3])[OH:2].[NH:4]([CH2:8][CH2:9][OH:10])[CH2:5][CH2:6][OH:7]

Participants

4

Reactant 3

HCID 280Carbon Dioxide2×HCID 962WaterHCID 8113Diethanolamine

Product 1

HCID 11499277HCID 11499277, compound

Procedure

Carbon dioxide was introduced into a mixture of diethanolamine (900 g=8.57 mol) and 80 g of water (4.44 mol) until saturation. In the course of 75 minutes, 73 l of CO2 (3.26 mol) were introduced into one sample and 72 l (3.21 mol) into another sample. The reaction temperature rose to 63° C. without cooling.

Workup

  1. customrose to 63° C.
  2. temperaturewithout cooling

Sources & evidence

ORD record
ord-22e5599b88b548b5ab347725ae42fb2c
Source dataset
uspto-grants-1985_02
Patent number
US04500656

Reaction notes

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