Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | 2-Phenoxycarbonylaminothiazolo[4,5-c]pyridine | HCID 15593549 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 15593550 | HCID 15593550 | 98% |
Reaction Steps
A mixture of 2-phenoxycarbonylaminothiazolo[4,5-c]-pyridine (200 mg, 0.73 mmole) and pyrrolidine (0.3 ml) in DMF (2 ml) was heated at 70° C. for 30 minutes and evaporated in vacuo. The residue was triturated with ether to give 180 mg (98%) of the desired product. Mp. 218°~220° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04500526 |
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| Source dataset | uspto-grants-1985_02 |
|---|
| ORD ID | ord-c7d78b2eca174240872e3d1a60ae52c3 |
|---|
| Source note | uspto-grants-1985_02 |
|---|
