Hydrochloric Acid → HCID 86739936, compound

HRID 615832Notes

Reaction equation

HRID 615832 reaction equation
[NH:1]([CH2:3][C:4]([OH:6])=[O:5])[CH3:2].[P:7]([OH:10])([OH:9])[OH:8].[ClH:11]>>[ClH:11].[CH3:2][N:1]([O:8][P:7]([CH2:3][C:4]([OH:6])=[O:5])([OH:10])=[O:9])[CH2:3][C:4]([OH:6])=[O:5]

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 1088SarcosineHCID 107909Phosphorous acid

Product 1

HCID 86739936HCID 86739936, compound

Procedure

In a like manner to Example 1, a solution of sarcosine (8.9 parts by weight), orthophosphorous acid (8.2 parts by weight) in 100 parts by weight of 18% hydrochloric acid is reacted to give, on evaporation, 25.8 parts by weight of 2-(N-methyl-N-carboxymethylamino)phosphonoacetic acid hydrochloride as a pale yellow amorphous solid having a 31P-nmr signal at 13.3 ppm downfield from H3PO4 in water (JP-CH =18H3).

Sources & evidence

ORD record
ord-7bc2b629700a46a9886e84a138243bf9
Source dataset
uspto-grants-1985_02
Patent number
US04501667

Reaction notes

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