HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Hydroxy cyclopentyl-acetaldehyde → HCID 54157289, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Hydroxy cyclopentyl-acetaldehyde | HCID 53769794 | — |
| Catalyst | Butyltriphenylphosphonium bromide | HCID 159628 | — |
| Product | HCID 54157289 | HCID 54157289 | 42.7% |
Reaction Steps
Using the procedure of Example 3, 5 g of 3-hydroxy cyclopentyl-acetaldehyde and 20 g of triphenyl butyl phosphonium bromide were reacted and the product was chromatographed over silica gel. Elution with a 7-3 cyclohexane-ethyl acetate mixture yielded 1.4 g of 3-(2-hexenyl)-cyclopentanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04501687 |
| Source dataset | uspto-grants-1985_02 |
| ORD ID | ord-4cc7bc970b8749cb94668077f684ec93 |
| Source note | uspto-grants-1985_02 |