HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dicyclohexylcarbodiimide → N-[(3-pyridyl)methyl]-N-cyclohexyl-alpha-(n-butylthio)acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | (Butylthio)acetic acid | HCID 88607 | — |
| Reactant | N-(pyridin-3-ylmethyl)cyclohexanamine | HCID 757273 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | N-[(3-pyridyl)methyl]-N-cyclohexyl-alpha-(n-butylthio)acetamide | HCID 13652431 | — |
Reaction Steps
N-[(3-pyridyl)methyl]-N-cyclohexyl-α-(n-butylthio)acetamide was prepared by the method of Example 2 by reacting 9.5 g. of N-cyclohexyl-[(3-pyridyl)methyl]amine with 7.4 g. of α-(n-butylthio)acetic acid and 9.0 g. of N,N'-dicyclohexylcarbodiimide in 150 ml of toluene. Weight 3.5 g. as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04501746 |
| Source dataset | uspto-grants-1985_02 |
| ORD ID | ord-a3b3d36ee45348c6a1c737e25c9656d8 |
| Source note | uspto-grants-1985_02 |