HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dicyclohexylcarbodiimide → N-[1-(3-pyridyl)ethyl]-N-cyclohexyl-alpha-(n-butylthio)acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | (Butylthio)acetic acid | HCID 88607 | — |
| Reactant | N-cyclohexyl-[1-(3-pyridyl)ethyl]amine | HCID 20406780 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | N-[1-(3-pyridyl)ethyl]-N-cyclohexyl-alpha-(n-butylthio)acetamide | HCID 20406784 | — |
Reaction Steps
N-[1-(3-pyridyl)ethyl]-N-cyclohexyl-α-(n-butylthio)acetamide was prepared by the method of Example 2 by reacting 5.0 g. of N-cyclohexyl-[1-(3-pyridyl)ethyl]amine with 3.6 g. of α-(n-butylthio)acetic acid and 5.0 g. of N,N'-dicyclohexylcarbodiimide in 200 ml. of dichloromethane. Oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04501746 |
| Source dataset | uspto-grants-1985_02 |
| ORD ID | ord-eb5066fbc0a64bc08691906e4fbb2049 |
| Source note | uspto-grants-1985_02 |