HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dicyclohexylcarbodiimide → N-(1-methylhexyl)-N-[(3-pyridyl)methyl]-alpha-(n-butylthio)acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | (Butylthio)acetic acid | HCID 88607 | — |
| Reactant | 3-(1-Methylhexylaminomethyl)pyridine | HCID 14720282 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | N-(1-methylhexyl)-N-[(3-pyridyl)methyl]-alpha-(n-butylthio)acetamide | HCID 13652437 | — |
Reaction Steps
N-(1-methylhexyl)-N-[(3-pyridyl)methyl]-α-(n-butylthio)acetamide was prepared by the method of Example 2 by reacting 3.6 g. of α-(n-butylthio)acetic acid and 5.0 g. of N,N'-dicyclohexylcarbodiimide with 5.0 g. of N-(1-methylhexyl)-[(3-pyridyl)methyl]amine in 200 ml. of dichloromethane. Oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04501746 |
| Source dataset | uspto-grants-1985_02 |
| ORD ID | ord-8f1acc1d91fe4a60b4cd80e3e92366a2 |
| Source note | uspto-grants-1985_02 |