HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 13652438, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | 4-chloro-N-(pyridin-3-ylmethyl)aniline | HCID 2804545 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 13652438 | HCID 13652438 | — |
Reaction Steps
N-[(3-pyridyl)methyl]-N-(4-chlorophenyl)acetamide was prepared by reacting 5.0 g. of N-(4-chlorophenyl)-[(3-pyridyl)methyl]amine with 2.0 g. of acetyl chloride in 250 ml. containing 3.0 g. of triethylamine according to the method of Example 11. Weight 1.1 g. M.P. 64°-65° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04501746 |
| Source dataset | uspto-grants-1985_02 |
| ORD ID | ord-7d573c15305c45d1b1fd9e6b12a67a52 |
| Source note | uspto-grants-1985_02 |