HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl chloroformate → HCID 18998995, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 1,6-Bis(2,2,6,6-tetramethyl-4-piperidylamino)hexane | HCID 93419 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 18998995 | HCID 18998995 | — |
Reaction Steps
The N,N'-bis-(ethoxycarbonyl)-N,N'-bis-(2,2,6,6-tetramethyl-piperidin-4-yl)-hexamethylenediamine was prepared by reacting N,N'-bis-(2,2,6,6-tetramethyl-piperidin-4-yl)-hexamethylenediamine with ethyl chlorocarbonate in toluene in the presence of aqueous NaOH and was crystallised from octane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04501837 |
| Source dataset | uspto-grants-1985_02 |
| ORD ID | ord-75a852042da1470b858a622f8fc14518 |
| Source note | uspto-grants-1985_02 |