HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 54539334, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Glycidol | HCID 11164 | — |
| Reactant | Methyl [4-(chlorocarbonyl)phenyl]acetate | HCID 20406944 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 54539334 | HCID 54539334 | — |
Reaction Steps
A mixture containing 14.8 g (0.2 mole) of glycidol, 150 ml of anhydrous ether, 16 g (0.4 mole of pyridine and 43 g (0.2 mole) of 4-[(methoxycarbonyl)methyl]benzoyl chloride is stirred at room temperature for two hours. The mixture is filtered and the ether evaporated to leave an oil. This oil is distilled to give a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04501912 |
| Source dataset | uspto-grants-1985_02 |
| ORD ID | ord-b684324242e74d78bcd633169f3c09aa |
| Source note | uspto-grants-1985_02 |