Iodoethane → HCID 20370364, compound

HRID 615973Notes

Reaction equation

HRID 615973 reaction equation
[CH3:1][N:2]([CH3:19])[C:3](=[O:18])[CH:4]([CH3:17])[N:5]1[CH:9]=[C:8]([CH3:10])[C:7]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)=[N:6]1.[CH2:20](I)[CH3:21]>>[CH3:19][N:2]([CH3:1])[C:3]([C:4]1([N:5]2[CH:9]=[C:8]([CH3:10])[C:7]([C:11]3[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=3)=[N:6]2)[CH2:21][CH2:20][CH2:17]1)=[O:18]

Participants

3

Reactant 2

HCID 6340IodoethaneHCID 20370501N,N-Dimethyl-2-(4-methyl-3-phenyl-1H-pyrazol-1-yl)propanamide

Product 1

HCID 20370364HCID 20370364, compound

Procedure

Following the procedure of Example 95, but substituting α-(3-bromopropyl)-N,N,4-trimethyl-3-phenylpyrazole-1-acetamide for N,N,α,4-tetramethyl-3-phenylpyrazole-1-acetamide and without the addition of ethyl iodide there was obtained N,N-dimethyl-1-(4-methyl-3-phenylpyrazol-1-yl)cyclobutanecarboxamide having a melting point of 87°-89° C.

Sources & evidence

ORD record
ord-12082881c27444e58bb80586e0a119e8
Source dataset
uspto-grants-1978_02
Patent number
US04072498

Reaction notes

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