HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-N,N,2-trimethylpropanamide → N,N,beta,4-tetramethyl-3-phenylpyrazole-1-propionamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-N,N,2-trimethylpropanamide | HCID 12475644 | — |
| Reactant | HCID 178420101 | HCID 178420101 | — |
| Reactant | HCID 178430907 | HCID 178430907 | — |
| Product | N,N,beta,4-tetramethyl-3-phenylpyrazole-1-propionamide | HCID 20370400 | — |
| Product | alpha-ethyl-N,N,4-trimethyl-3-phenylpyrazole-1-acetamide | HCID 20568045 | — |
Reaction Steps
Following the procedure of Example 121, but substituting 2-bromo-N,N-dimethylbutyramide for 2-bromo-N,N,2-trimethylpropionamide, and 4-methyl-3-phenylpyrazole for 3-phenylpyrazole, there were obtained the already described α-ethyl-N,N,4-trimethyl-3-phenylpyrazole-1-acetamide and N,N,β,4-tetramethyl-3-phenylpyrazole-1-propionamide having a boiling point of 170°/0.2 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04072498 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-2349013dd8084e758478cf9cb2b197d1 |
| Source note | uspto-grants-1978_02 |