Methyl iodide → HCID 20370520, compound

HRID 615992Notes

Reaction equation

HRID 615992 reaction equation
[CH3:1][N:2]([CH3:19])[C:3](=[O:18])[CH:4]([CH3:17])[N:5]1[CH:9]=[C:8]([CH3:10])[C:7]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)=[N:6]1.[CH3:20]I.[CH2:22](I)[CH3:23]>>[CH3:19][N:2]([CH3:1])[C:3](=[O:18])[C:4]([CH3:20])([CH3:17])[N:5]1[CH:9]=[C:8]([CH2:10][CH2:22][CH3:23])[C:7]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)=[N:6]1

Participants

4

Reactant 3

HCID 6328Methyl iodideHCID 6340IodoethaneHCID 20370501N,N-Dimethyl-2-(4-methyl-3-phenyl-1H-pyrazol-1-yl)propanamide

Product 1

HCID 20370520HCID 20370520, compound

Procedure

Following the procedure of Example 95, but substituting N,N,α-trimethyl-3-phenyl-4-propylpyrazole-1-acetamide for N,N,α,4-tetramethyl-3-phenypyrazole-1-acetamide and methyl iodide for ethyl iodide, there was obtained N,N,α,α-tetramethyl-3-phenyl-4-propylpyrazole-1-acetamide, m.p. 98.5°-101° C.

Sources & evidence

ORD record
ord-2b94a09c5abd436f98c43ea802aa1b01
Source dataset
uspto-grants-1978_02
Patent number
US04072498

Reaction notes

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