HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → 2-Nitro-4-(propane-1-sulfinyl)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 20371008 | HCID 20371008 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2-Nitro-4-(propane-1-sulfinyl)aniline | HCID 20362825 | — |
Reaction Steps
1.5 G. of 1-acetamido-2-nitro-4-n-propylsulfinylbenzene is treated with 3 ml. of 5N sodium hydroxide solution and sufficient methanol to effect solution. After heating on a steam bath for 15 minutes, the mixture is diluted with water, cooled and filtered, yielding 1-amino-2-nitro-4-n-propylsulfinylbenzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04072696 |
| Source dataset | uspto-grants-1978_02 |
| ORD ID | ord-d4453324c7444c0da936d3fe495a7343 |
| Source note | uspto-grants-1978_02 |