Methoxycarbonyl isothiocyanate → HCID 20371180, compound

Participants

Reaction Steps

2.6 G. 1,2-diamino-4-thiocyanatobenzene in 48 ml. acetone is treated overnight with 8 g. methoxy carbonyl isothiocyanate at room temperature. The solution is concentrated and the residue triturated with methanol and recrystallized from methanol-chloroform, yielding pure 1,2-bis-(3-methoxycarbonyl-2-thioureido)-4-thiocyanatobenzene.

Provenance & Evidence